I-5-nitroisophthalic acid
Indawo yokunyibilika: 259-261 °C(lit.)
Indawo yokubila: 350.79°C (uqikelelo olurhabaxa)
Ubuninzi: 1.6342 (uqikelelo olurhabaxa)
Isalathiso se-refractive: 1.5282 (uqikelelo)
Indawo edanyazayo: 120°C
Ukunyibilika: Ukunyibilika etywaleni, ether nakumanzi ashushu
iimpawu: umhlophe kumgubo omhlophe.
Uxinzelelo lomphunga: 0.0±1.2 mmHg ku-25°C
iinkcukacha | iyunithi | umgangatho |
Imbonakalo | Imhlophe ukuya kumgubo omhlophe | |
Umxholo | % | ≥99% |
Ukufuma | % | ≤0.5 |
Isiphakathi esibalulekileyo sokusasaza idayi. Ikwayindawo ephakathi kwiyeza lokuxilonga i-ubiquitin entsha (i-X-reyi yokuthelekisa i-agent); Ikwasetyenziselwa ukudibanisa i-compound yeziyobisi ezinoveli ngokusekelwe kwi-PDE IV inhibitor glycolinic acid; Ikwasetyenziswa njengendawo ephakathi yokusasaza idayi (i-azo dyes eluhlaza okwesibhakabhaka).
I-asidi ye-sulfuric egxininisiweyo (104.3mL, 1.92mol) yongezwa kwiibhotile ezintathu, emva koko isophthalic acid (40g, 0.24mol) yongezwa, ixutywe kwaye ishushu kwi-60 ℃, ibanjwe i-0.5h, kunye ne-60% ye-nitric acid (37.8g, 0.36) mol) yongezwa ukulawula iqondo lokukhawulezisa amathontsi. Yongeza kwiiyure ezi-2. Emva koko, ukusabela kokugcina ubushushu kwi-60 ℃ kwiiyure ezi-2. Phola ukuya ngaphantsi kwe 50 ° C, emva koko wongeze i-100mL yamanzi. Izinto eziphathekayo zipholile kwiqondo lokushisa, zithululelwe kwisihlunu, zixutywe ukuze zisuse i-asidi yenkunkuma, ikhekhe lokucoca lihlanjwe ngamanzi, lihlanjululwe ukuze lihlaziye, kwaye imveliso emhlophe yayiyi-34.6 grams, isivuno sasiyi-68.4%.
I-25kg / i-3-in-1 ye-paper-plastic composite bag, okanye isikhwama esilukiweyo, okanye i-25kg / ibhakethi yekhadibhodi (φ410 × 480mm); Ukupakishwa ngokweemfuno zabathengi;
Gcina kwisingxobo esingangeni moya kwindawo epholileyo, eyomileyo, nengena umoya kakuhle kude nomlilo nezinto ezinokutsha.